(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Base Information

Chemical Name:(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide
CAS No.:1265608-65-8
Molecular Formula:C₁₈H₂₀N₂O₆
Molecular Weight:360.367
Hs Code.:

Synonyms:(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Suppliers and Price of (2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Chemical Property:

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Technology Process of (2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

There total 3 articles about (2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 121-33-5,8014-42-4
vanillin

: 3291-03-0
3,4,5-trimethoxybenzohydrazide

: 1265608-65-8
(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Guidance literature:: In methanol; for 2h; Reflux;
DOI:10.1590/S0103-50532010000100021

Reference yield:

: 1916-07-0
3,4,5-trimethoxybenzoic acid methyl ester

: 1265608-65-8
(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol / 20 °C / Reflux

2: methanol / 2 h / Reflux

With hydrazine hydrate; In methanol;
DOI:10.1016/j.ejmech.2015.02.041

Reference yield:

: 149-91-7
3,4,5-trihydroxybenzoic acid

: 1265608-65-8
(2E)-N'-(4'-hydroxy-5'-methoxybenzylidene)-3,4,5-trimethoxybenzohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetone / 12 h / Reflux

2: hydrazine hydrate / methanol / 20 °C / Reflux

3: methanol / 2 h / Reflux

With tetra-(n-butyl)ammonium iodide; potassium carbonate; hydrazine hydrate; In methanol; acetone;
DOI:10.1016/j.ejmech.2015.02.041