rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

Base Information

Chemical Name:rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane
CAS No.:909576-67-6
Molecular Formula:C₁₇H₃₀N₂Si
Molecular Weight:290.524
Hs Code.:

Synonyms:rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

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Chemical Property of rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

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Technology Process of rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

There total 4 articles about rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 909576-66-5
1-(1-phenylvinyl)-1-silacyclohexane

: 124-40-3
dimethyl amine

: 1,1-bis(dimethylamino)-1-silacyclohexane

: 909576-67-6
rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

: 1126-71-2
N,N-dimethylphenethylamine

Guidance literature:: dimethyl amine; With n-butyllithium; In tetrahydrofuran; hexane; at -50 - -12 ℃; for 2h;

1-(1-phenylvinyl)-1-silacyclohexane; In tetrahydrofuran; hexane; at -30 - 4 ℃; for 19h;
DOI:10.1016/j.jorganchem.2006.04.015

Reference yield:

: 909576-65-4
1-methoxy-1-(1-phenylvinyl)-1-silacyclohexane

: 909576-67-6
rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 83 percent / lithium aluminium hydride / diethyl ether / 6.5 h / Heating

2.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -50 - -12 °C

2.2: 40 percent / hexane; tetrahydrofuran / 19 h / -30 - 4 °C

With lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/j.jorganchem.2006.04.015

Reference yield:

: 18141-41-8
1,1-dimethoxy-1-silacyclohexane

: 909576-67-6
rac-1-(dimethylamino)-1-[2-(dimethylamino)-1-phenylethyl]-1-silacyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / diethyl ether / 1 h / Heating

1.2: 59 percent / diethyl ether / 72 h / Heating

2.1: 83 percent / lithium aluminium hydride / diethyl ether / 6.5 h / Heating

3.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -50 - -12 °C

3.2: 40 percent / hexane; tetrahydrofuran / 19 h / -30 - 4 °C

With lithium aluminium tetrahydride; n-butyllithium; magnesium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/j.jorganchem.2006.04.015