5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

Base Information

Chemical Name:5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde
CAS No.:145640-33-1
Molecular Formula:C₂₄H₃₀O₂Si
Molecular Weight:381.563
Hs Code.:

Synonyms:5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

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Technology Process of 5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

There total 9 articles about 5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1-((tert-butyldiphenylsilyl)oxy)-4-(trideuteriomethyl)-3-((n-butylthio)methylidene)cyclohex-4-ene

: 145640-33-1
5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

Guidance literature:: With mercury dichloride; In water; acetonitrile; for 2h; Heating;
DOI:10.1021/jo00055a011

Reference yield:

: 41251-37-0
methyl-d3-magnesium iodide

: 4-((tert-butyldiphenylsilyl)oxy)-2-((n-butylthio)methylidene)cyclohexanone

: 145640-33-1
5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

Guidance literature:: With mercury dichloride; Yield given. Multistep reaction; 1) diethyl ether, a) -78 deg C, 10 min, b) 1 h without cooling bath, 2) CH₃CN, H₂O, reflux, 10 min;
DOI:10.1021/jo00055a011

Reference yield:

: 41251-37-0
methyl-d3-magnesium iodide

: 4-(tert-butyldiphenylsilyloxy)-2-<2'-(1',3'-dioxanyl)>cyclohexane

: 145640-33-1
5-((tert-butyldiphenylsilyl)oxy)-2-(trideuteriomethyl)cyclohex-1-enecarboxaldehyde

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1) ether, a) 0 deg C, 10 min, b) room temperature, 1 h, 2) acetone, heating;
DOI:10.1021/jo00055a011