2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

Base Information

Chemical Name:2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene
CAS No.:67887-87-0
Molecular Formula:C₃₂H₂₄FeP₂
Molecular Weight:526.337
Hs Code.:

Synonyms:2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

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Chemical Property of 2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

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Technology Process of 2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

There total 1 articles about 2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1162-70-5
1,2,5-triphenyl-1H-phosphole

: iron(II) chloride

: 67887-87-0
2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

Guidance literature:: With Li; In tetrahydrofuran; byproducts: (C6H5)2; Ar, soln. of Li and the phosphole stirred at room temp. for 5 h, filtered, FeCl2 added to the filtrate, stirred at room temp. for 12 h then refluxed for 1 h; evapd. to dryness, extrd. (benzene), extract chromd. (hexane/benzene (80/20)); elem. anal.;
DOI:10.1021/ja00523a015

Reference yield: 80.0%

: 67887-87-0
2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

: 2966-50-9
silver trifluoroacetate

: 106923-20-0
(PC₄H₂(C₆H₅)2)2FeAgOCOCF₃

Guidance literature:: In acetone; under Ar: suspending of 0.57 mmol (PC4H2(C6H5)2)2Fe in dry acetone soln. of 0.57 mmol silver trifluoroacetate; stirring at room temperature for1 h; pptn.;; filtration; washing with acetone; elem. anal.;;
DOI:10.1016/S0020-1693(00)84335-2

Reference yield: 71.0%

: 67887-87-0
2,2',5,5'-tetraphenyl-1,1'-diphosphaferrocene

: 2923-28-6
silver trifluoromethanesulfonate

: 106923-18-6
2,2',5,5'-tetraphenyldiphosphaferrocene/silver triflate complex

Guidance literature:: In benzene; under Ar: dissolving of 0.38 mmol (PC4H2(C6H5)2)2Fe in benzene; filtration; addn. of 0.38 mmol silver triflate; stirring for 0.5 h; storing for1 h; pptn.;; filtration; washing with dry benzene; drying in vac.; elem. anal.;;
DOI:10.1016/S0020-1693(00)84335-2