(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

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Chemical Name:(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol
CAS No.:347852-06-6
Molecular Formula:C₁₉H₃₄O₆
Molecular Weight:358.475
Hs Code.:

Synonyms:(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

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Chemical Property of (2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

There total 3 articles about (2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 347852-09-9
C₄₇H₅₀O₁₀

: 347852-06-6
(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With ammonia; In methanol; at 20 ℃; for 24h;
DOI:10.1016/S0031-9422(00)00361-7

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 347852-06-6
(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 mg / Hg(CN)2; 4 Angstroem molecular sieves / acetonitrile / 36 h / 20 °C

2: 90 percent / NH₃ / methanol / 24 h / 20 °C

With 4 A molecular sieve; ammonia; mercury(II) cyanide; In methanol; acetonitrile; 1: Koenigs-Knorr reaction;
DOI:10.1016/S0031-9422(00)00361-7

Reference yield:

: 7,8-dihydro-α-ionol

: 347852-06-6
(2R,3S,4S,5R,6R)-2-Hydroxymethyl-6-[(R)-1-methyl-3-(2,6,6-trimethyl-cyclohex-2-enyl)-propoxy]-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 mg / Hg(CN)2; 4 Angstroem molecular sieves / acetonitrile / 36 h / 20 °C

2: 90 percent / NH₃ / methanol / 24 h / 20 °C

With 4 A molecular sieve; ammonia; mercury(II) cyanide; In methanol; acetonitrile; 1: Koenigs-Knorr reaction;
DOI:10.1016/S0031-9422(00)00361-7