ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

Base Information

Chemical Name:ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate
CAS No.:616236-31-8
Molecular Formula:C₃₁H₄₃NO₆
Molecular Weight:525.686
Hs Code.:

Synonyms:ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

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Chemical Property of ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

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Technology Process of ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

There total 7 articles about ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 616236-30-7
6-[4-(2,4-dihydroxy-3,3-dimethylbutyrylamino)-3,5-dimethylphenoxy]-2,2-dimethylhexanoic acid ethyl ester

: 1125-88-8
benzaldehyde dimethyl acetal

: 616236-31-8
ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 20h;
DOI:10.1080/00397910500377545

Reference yield:

: 3-(1-ethoxy-ethoxy)-4,4-dimethyl-dihydro-furan-2-one

: 616236-31-8
ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / NaH / dimethylformamide / 6 h

2: 76 percent / HOAc / H₂O / 4 h

3: 95 percent / TsOH*H₂O / CH₂Cl₂ / 20 h

With sodium hydride; toluene-4-sulfonic acid; acetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545

Reference yield:

: 616236-28-3
6-(4-amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid ethyl ester

: 616236-31-8
ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / NaH / dimethylformamide / 6 h

2: 76 percent / HOAc / H₂O / 4 h

3: 95 percent / TsOH*H₂O / CH₂Cl₂ / 20 h

With sodium hydride; toluene-4-sulfonic acid; acetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545