6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

Base Information

Chemical Name:6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid
CAS No.:616236-32-9
Molecular Formula:C₂₉H₃₉NO₆
Molecular Weight:497.632
Hs Code.:

Synonyms:6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

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Chemical Property of 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

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Technology Process of 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

There total 8 articles about 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 616236-31-8
ethyl 6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoate

: 616236-32-9
6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

Guidance literature:: With lithium hydroxide; In ethanol; water; for 38h; Heating;
DOI:10.1080/00397910500377545

Reference yield:

: 3-(1-ethoxy-ethoxy)-4,4-dimethyl-dihydro-furan-2-one

: 616236-32-9
6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 39 percent / NaH / dimethylformamide / 6 h

2: 76 percent / HOAc / H₂O / 4 h

3: 95 percent / TsOH*H₂O / CH₂Cl₂ / 20 h

4: 97 percent / LiOH / ethanol; H₂O / 38 h / Heating

With lithium hydroxide; sodium hydride; toluene-4-sulfonic acid; acetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545

Reference yield:

: 616236-28-3
6-(4-amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid ethyl ester

: 616236-32-9
6-(4-[(5,5-dimethyl-2-phenyl-1,3-dioxan-4-yl)carbonyl]amino-3,5-dimethylphenoxy)-2,2-dimethylhexanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 39 percent / NaH / dimethylformamide / 6 h

2: 76 percent / HOAc / H₂O / 4 h

3: 95 percent / TsOH*H₂O / CH₂Cl₂ / 20 h

4: 97 percent / LiOH / ethanol; H₂O / 38 h / Heating

With lithium hydroxide; sodium hydride; toluene-4-sulfonic acid; acetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1080/00397910500377545