1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

Base Information

Chemical Name:1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone
CAS No.:1289579-39-0
Molecular Formula:C₂₂H₁₆ClNOS₂
Molecular Weight:409.96
Hs Code.:

Synonyms:1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

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Chemical Property of 1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

Chemical Property:

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Technology Process of 1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

There total 1 articles about 1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 75-15-0,12122-00-8
carbon disulfide

: 100-39-0
benzyl bromide

: 133303-48-7
2-(p-chlorobenzyl)-1-(ethoxycarbonylmethyl)pyridinium bromide

: 1289579-39-0
1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

Guidance literature:: 2-(p-chlorobenzyl)-1-(ethoxycarbonylmethyl)pyridinium bromide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; at 60 ℃; for 0.25h;

carbon disulfide; In ethanol; at 20 ℃; for 0.25h;

benzyl bromide; In ethanol; at 20 ℃; for 1.5h;
DOI:10.3987/COM-10-S(E)72

Reference yield: 59.0%

: 1289579-39-0
1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

: 105-36-2
ethyl bromoacetate

: ethyl 3-benzylthio-5-(p-chlorophenyl)-4-oxo-1H-8,8a-dihydro-1,4-thiazino[3,4,5-cd]indolizine-1-carboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 50 ℃; for 0.166667h; optical yield given as %de;
DOI:10.3987/COM-10-S(E)72

Reference yield:

: 1289579-39-0
1-(p-chlorophenyl)-(Z)-3-[(benzylthio)mercaptomethylene]-2(3H)-indolizinone

: 1289579-98-1
ethyl 4-(p-chlorophenyl)-2-benzylthio-3-hydroxycyclo[3.2.2]azine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / chloroform / 0.17 h / 50 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 2,4,6-trimethyl-pyridine / 0.25 h / 180 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 2,4,6-trimethyl-pyridine; chloroform;
DOI:10.3987/COM-10-S(E)72