N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine

Base Information

• Chemical Name: N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine
• CAS No.: 411208-44-1
• Molecular Formula: C₁₆H₁₆BrFN₂O₂S
• Molecular Weight: 399.284

Synonyms:N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine

Chemical Property of N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine

Chemical Property:

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Technology Process of N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine

There total 2 articles about N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

2-fluoroethyl bromide (762-49-2) + N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine (334632-66-5) → N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine (411208-44-1)

Guidance literature:

With triethylamine; In ethanol; at 70 ℃; for 16h;

DOI:10.1021/jm010939a

Reference yield:

N-methyl-2-(4-bromo-2-nitrophenylthio)benzamide (334632-65-4) → N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine (411208-44-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / B₂H₆ / tetrahydrofuran / 5 h / Heating

2: 46 percent / Et₃N / ethanol / 16 h / 70 °C

With triethylamine; diborane; In tetrahydrofuran; ethanol;

DOI:10.1021/jm010939a

Reference yield: 57.0%

N-(2-fluoroethyl)-N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine (411208-44-1) → N-(2-fluoroethyl),N-methyl-2-(2'-amino-4'-bromophenylthio)benzylamine

Guidance literature:

With hydrogenchloride; tin(ll) chloride; In methanol; at 20 ℃;

DOI:10.1021/jm010939a

upstream raw materials:

2-fluoroethyl bromide

N-methyl-2-(4'-bromo-2'-nitrophenylthio)benzylamine

N-methyl-2-(4-bromo-2-nitrophenylthio)benzamide

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