ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

Base Information

Chemical Name:ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate
CAS No.:1024010-93-2
Molecular Formula:CH₂O₂*C₁₄H₁₈N₂O₂
Molecular Weight:292.335
Hs Code.:

Synonyms:ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

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Chemical Property of ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

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Technology Process of ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

There total 7 articles about ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 64-18-6
formic acid

: 1024010-91-0
ethyl 4-((1R,4R)-5-benzyl-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate

: 1024010-93-2
ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

Guidance literature:: palladium on activated charcoal; In methanol; for 2h; Heating / reflux;

Reference yield:

: 61478-26-0
tert-butyl (2S,4R)-4-hydroxy-2-hydroxymethyl-pyrrolidine-1-carboxylate

: 1024010-93-2
ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 72 h / 0 °C

2: toluene / 18 h / 120 °C / Sealed tube

3: hydrogenchloride / 1,4-dioxane

4: dimethyl sulfoxide / 140 °C

5: palladium 10% on activated carbon / methanol / 2 h / Reflux

With pyridine; hydrogenchloride; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dimethyl sulfoxide; toluene;

Reference yield:

: tert-butyl 5-benzyl-2,5-diazabicyclo[2.2.1]heptane-2-carboxylate

: 1024010-93-2
ethyl 4-((1R,4R)-2,5-diazabicyclo[2.2.1]heptan-2-yl)benzoate formate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 1,4-dioxane

2: dimethyl sulfoxide / 140 °C

3: palladium 10% on activated carbon / methanol / 2 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dimethyl sulfoxide;