(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

Base Information

Chemical Name:(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione
CAS No.:1141896-00-5
Molecular Formula:C₂₉H₃₄N₂O₄
Molecular Weight:474.6
Hs Code.:

Synonyms:(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

There total 2 articles about (2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1470-99-1,1220913-24-5
cis-hexahydroisoindoline

: 1141895-98-8
(S)-3-benzyl-4-((R)-4-benzyl-2-oxooxazolidin-3-yl)-4-oxobutanoic acid

: 1141896-00-5
(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

Guidance literature:: (S)-3-benzyl-4-((R)-4-benzyl-2-oxooxazolidin-3-yl)-4-oxobutanoic acid; With triethylamine; In dichloromethane; at -30 - -20 ℃; for 0.25h;

With isobutyl chloroformate; In dichloromethane; at -30 - -20 ℃; for 1h;

cis-hexahydroisoindoline; In dichloromethane; at -30 - -20 ℃;

Reference yield:

: 1141896-00-5
(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

Guidance literature:: In methanol; at 0 - 5 ℃; for 5h; Purification / work up;

Reference yield:

: 1141896-00-5
(2S)-2-benzyl-1-((4R)-4-benzyl-2-oxo-oxazolidin-3-yl)-4-(cis-hexahydro-isoindolin-2-yl)-butane-1,4-dione

: 40217-17-2,90719-32-7,120574-96-1,102029-44-7
(R)-4-(phenylmethyl)-2-oxazolidinone

: 145375-43-5
mitiglinide

Guidance literature:: With lithium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 5 - 10 ℃; for 0.25h; Product distribution / selectivity;