7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Base Information

Chemical Name:7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane
CAS No.:107098-16-8
Molecular Formula:C₅₈H₇₂N₆O₁₃S₅
Molecular Weight:1221.57
Hs Code.:

Synonyms:7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Suppliers and Price of 7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

There total 3 articles about 7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 56187-04-3
1,4,7-tritosyl-1,4,7-triazaheptane

: 107098-12-4
9-benzoyl-6,12-bis(p-tolylsulfonyl)-1,17-bis(mesyloxy)-6,9,12-triaza-3,15-dioxaheptadecane

: 107098-16-8
7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 95 ℃; for 72h;
DOI:10.1021/jo00385a003

Reference yield:

: 77429-98-2
3-benzoyl-N¹,N⁵-ditosyl-3-azapentane-1,5-diamine

: 107098-16-8
7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / 72 h / 100 °C

2: 99 percent / triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

3: 55 percent / cesium carbonate / dimethylformamide / 72 h / 95 °C

With potassium carbonate; caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00385a003

Reference yield:

: 107098-11-3
9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

: 107098-16-8
7-benzoyl-4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

2: 55 percent / cesium carbonate / dimethylformamide / 72 h / 95 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00385a003