9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

Base Information

Chemical Name:9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol
CAS No.:107098-11-3
Molecular Formula:C₃₃H₄₅N₃O₉S₂
Molecular Weight:691.867
Hs Code.:

Synonyms:9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

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Chemical Property of 9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

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Technology Process of 9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

There total 1 articles about 9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77429-98-2
3-benzoyl-N¹,N⁵-ditosyl-3-azapentane-1,5-diamine

: 628-89-7
2-(2-Chloroethoxy)ethanol

: 107098-11-3
9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

Guidance literature:: With potassium carbonate; at 100 ℃; for 72h;
DOI:10.1021/jo00385a003

Reference yield: 99.0%

: 124-63-0
methanesulfonyl chloride

: 107098-11-3
9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

: 107098-12-4
9-benzoyl-6,12-bis(p-tolylsulfonyl)-1,17-bis(mesyloxy)-6,9,12-triaza-3,15-dioxaheptadecane

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00385a003

Reference yield:

: 107098-11-3
9-benzoyl-6,12-bis(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diol

: 107098-17-9
4,10,16,19,22-pentakis(p-tolylsulfonyl)-1,13-dioxa-4,7,10,16,19,22-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

2: 55 percent / cesium carbonate / dimethylformamide / 72 h / 95 °C

3: 82 percent / water, potassium tert-butoxide / tetrahydrofuran / 1 h / Heating

With potassium tert-butylate; water; caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00385a003