2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

Base Information

Chemical Name:2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate
CAS No.:93206-06-5
Molecular Formula:C₁₅H₁₇N₅O₅
Molecular Weight:347.33
Hs Code.:

Synonyms:2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

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Chemical Property of 2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

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Technology Process of 2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

There total 2 articles about 2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 93206-05-4
<2-(benzoyloxy)ethoxy>acetic acid

: 93206-04-3
3-amino-6-(aminomethyl)-1,2,4-triazin-5(4H)-one hydrochloride

: 93206-06-5
2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

Guidance literature:: With sodium hydroxide; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In water; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570210313

Reference yield:

: 20587-61-5
diethylene glycol benzoate

: 93206-06-5
2-<<<(3-amino-4,5-dihydro-5-oxo-1,2,4-triazin-6-yl)methylamino>carbonyl>methoxy>ethanol benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / Jones reagent / acetone / 18 h / Ambient temperature

2: 43 percent / 2N NaOH, N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / H₂O / 3 h / 70 °C

With sodium hydroxide; jones reagent; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In water; acetone;
DOI:10.1002/jhet.5570210313