Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)-

Base Information

Chemical Name:Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)-
CAS No.:944828-13-1
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:
Mol file:944828-13-1.mol

Synonyms:Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)-

Chemical Property:

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Technology Process of Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)-

There total 5 articles about Ethanone, 1-(1,2-dihydrospiro[cyclopropane-1,3-[3H]indol]-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 115802-65-8
N-(2-methylprop-2-en-1-yl)-2-bromoacetanilide

: 944828-13-1
N-acetyl-1',2'-dihydrospiro[cyclopropane-1,3'-indoline]

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; Trimethylacetic acid; In dimethyl sulfoxide; at 120 ℃; regioselective reaction; Inert atmosphere; Molecular sieve; Glovebox;
DOI:10.1002/anie.201809133

Reference yield: 71.0%

: 115802-65-8
N-(2-methylprop-2-en-1-yl)-2-bromoacetanilide

: 944828-13-1
N-acetyl-1',2'-dihydrospiro[cyclopropane-1,3'-indoline]

: 1-(6b-methyl-1,6b-dihydrocyclopropa[b]indol-2(1aH)-yl)ethanone

: 16078-32-3
1-(3,3-dimethylindolin-1-yl)ethan-1-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; Trimethylacetic acid; In dimethyl sulfoxide; at 120 ℃; for 24h; Solvent; regioselective reaction; Catalytic behavior; Inert atmosphere;
DOI:10.1002/anie.201809133

Reference yield: 50.0%

: 115802-65-8
N-(2-methylprop-2-en-1-yl)-2-bromoacetanilide

: 944828-13-1
N-acetyl-1',2'-dihydrospiro[cyclopropane-1,3'-indoline]

: 16078-32-3
1-(3,3-dimethylindolin-1-yl)ethan-1-one

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; triphenylphosphine; palladium diacetate; In N,N-dimethyl-formamide; at 120 ℃;
DOI:10.1016/j.tetlet.2007.05.018