4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

Base Information

Chemical Name:4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile
CAS No.:108365-46-4
Molecular Formula:C₃₄H₄₉ClN₂O₉
Molecular Weight:665.224
Hs Code.:

Synonyms:4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

Chemical Property:

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Technology Process of 4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

There total 9 articles about 4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 7677-24-9
trimethylsilyl cyanide

: 121784-63-2
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

: 108365-46-4
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

: 120255-37-0
2,2-Dimethyl-propionic acid (2R,3R,4S,5S,6R)-2-{[(S)-(4-chloro-phenyl)-cyano-methyl]-amino}-3,5-bis-(2,2-dimethyl-propionyloxy)-6-(2,2-dimethyl-propionyloxymethyl)-tetrahydro-pyran-4-yl ester

Guidance literature:: With tin(IV) chloride; In tetrahydrofuran; at -60 - -10 ℃; for 6h; Yields of byproduct given;

Reference yield: 84.0%

: 7677-24-9
trimethylsilyl cyanide

: 121784-63-2
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)benzylideneamine

: 108365-46-4
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

Guidance literature:: With tin(IV) chloride; In tetrahydrofuran; at -18 ℃; for 6h;

Reference yield:

: 108342-86-5
2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl azide

: 108365-46-4
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-D-phenylglycinotrile

Guidance literature:: Multi-step reaction with 3 steps

1: H₂

2: glacial acetic acid / propan-2-ol

3: 84 percent / SnCl₄ / tetrahydrofuran / 6 h / -60 - -10 °C

With hydrogen; tin(IV) chloride; acetic acid; In tetrahydrofuran; isopropyl alcohol;