C₂₄H₂₈O₇

Base Information

Chemical Name:C₂₄H₂₈O₇
CAS No.:114828-03-4
Molecular Formula:C₂₄H₂₈O₇
Molecular Weight:428.482
Hs Code.:

C<sub>24</sub>H<sub>28</sub>O<sub>7</sub>

Synonyms:C₂₄H₂₈O₇

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Chemical Property of C₂₄H₂₈O₇

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Technology Process of C₂₄H₂₈O₇

There total 21 articles about C₂₄H₂₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 124516-70-7
C₂₉H₄₀O₇Si

: 114828-03-4
C₂₄H₂₈O₇

Guidance literature:: With tetra(tert-butyl)-ammonium fluoride; In dimethyl sulfoxide; at 50 ℃; for 2h;

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 114828-03-4
C₂₄H₂₈O₇

Guidance literature:: Multi-step reaction with 16 steps

1: 100 percent / p-TsOH*H₂O / benzene / 1 h / Heating

2: 91 percent / pyridinium bromide perbromide / tetrahydrofuran / 0.25 h / Ambient temperature

3: 77 percent / t-BuOK / dimethylsulfoxide / 0.25 h / Ambient temperature

4: 1.) t-BuLi, 2.) HMPA / 1.) THF, pentane, 0 deg C, 1 h, 2.) THF, pentane, -78 deg C, 30 min

5: oxalic acid / CH₂Cl₂ / 2 h / Ambient temperature

6: (COCl)2, DMSO / CH₂Cl₂ / 0.5 h / -78 °C

7: ZnBr₂ / CH₂Cl₂ / 23 h / Ambient temperature

8: camphorsulfonic acid (CSA) / benzene / 18 h / Ambient temperature

9: 79 percent / dimethylsulfoxide; tetrahydrofuran / 1.75 h / 0 - 20 °C

11: 229.4 mg / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 0.67 h / Ambient temperature

12: 82 percent / NaIO₄, RuCl₃ / H₂O; CCl₄; acetonitrile / 3 h / Ambient temperature

13: 83 percent / 1,3-dicyclohexylcarbodiimide, 4-pyrrolidinopyridine / CH₂Cl₂ / 1 h / Ambient temperature

14: 80 percent / NaBH₄ / methanol; tetrahydrofuran / 0.67 h / -30 °C

15: 94 percent / 4-pyrrolidinopyridine, Et₃N / pyridine / 48 h / Ambient temperature

16: 91 percent / t-Bu₄NF / dimethylsulfoxide / 2 h / 50 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; oxalyl dichloride; camphor-10-sulfonic acid; potassium tert-butylate; hydrogen; tert.-butyl lithium; pyridinium hydrobromide perbromide; oxalic acid; 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; dimethyl sulfoxide; tetra(tert-butyl)-ammonium fluoride; triethylamine; dicyclohexyl-carbodiimide; zinc dibromide; palladium dihydroxide; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;

Reference yield:

: 3592-25-4
1,5-dichloropentan-3-one

: 114828-03-4
C₂₄H₂₈O₇

Guidance literature:: Multi-step reaction with 17 steps

1: 35 percent / aq. NaH₂PO₄, o-H₃PO₄ / 3 h / 100 °C

2: 100 percent / p-TsOH*H₂O / benzene / 1 h / Heating

3: 91 percent / pyridinium bromide perbromide / tetrahydrofuran / 0.25 h / Ambient temperature

4: 77 percent / t-BuOK / dimethylsulfoxide / 0.25 h / Ambient temperature

5: 1.) t-BuLi, 2.) HMPA / 1.) THF, pentane, 0 deg C, 1 h, 2.) THF, pentane, -78 deg C, 30 min

6: oxalic acid / CH₂Cl₂ / 2 h / Ambient temperature

7: (COCl)2, DMSO / CH₂Cl₂ / 0.5 h / -78 °C

8: ZnBr₂ / CH₂Cl₂ / 23 h / Ambient temperature

9: camphorsulfonic acid (CSA) / benzene / 18 h / Ambient temperature

10: 79 percent / dimethylsulfoxide; tetrahydrofuran / 1.75 h / 0 - 20 °C

12: 229.4 mg / H₂ / 10percent Pd(OH)2/C / ethyl acetate / 0.67 h / Ambient temperature

13: 82 percent / NaIO₄, RuCl₃ / H₂O; CCl₄; acetonitrile / 3 h / Ambient temperature

14: 83 percent / 1,3-dicyclohexylcarbodiimide, 4-pyrrolidinopyridine / CH₂Cl₂ / 1 h / Ambient temperature

15: 80 percent / NaBH₄ / methanol; tetrahydrofuran / 0.67 h / -30 °C

16: 94 percent / 4-pyrrolidinopyridine, Et₃N / pyridine / 48 h / Ambient temperature

17: 91 percent / t-Bu₄NF / dimethylsulfoxide / 2 h / 50 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; sodium dihydrogenphosphate; oxalyl dichloride; phosphoric acid; camphor-10-sulfonic acid; potassium tert-butylate; hydrogen; tert.-butyl lithium; pyridinium hydrobromide perbromide; oxalic acid; 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; dimethyl sulfoxide; tetra(tert-butyl)-ammonium fluoride; triethylamine; dicyclohexyl-carbodiimide; zinc dibromide; palladium dihydroxide; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; acetonitrile; benzene;