4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine)

Base Information

Chemical Name:4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine)
CAS No.:99305-42-7
Molecular Formula:C23H42 N2 O4
Molecular Weight:410.597
Hs Code.:2924299090
European Community (EC) Number:619-422-7
DSSTox Substance ID:DTXSID90893706
Nikkaji Number:J1.227.815B

Synonyms:4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine);99305-42-7;EC 619-422-7;SCHEMBL1111487;DTXSID90893706;NS00007890

Suppliers and Price of 4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine)

Chemical Property:

Boiling Point:543.3±17.0 °C (760 mmHg)
PSA：76.66000
Density:1.04±0.1 g/cm3 (20 °C, 760 mmHg)
LogP:6.32850
Solubility.:24.5g/L in organic solvents at 20 ℃
Water Solubility.:78μg/L at 20℃
XLogP3:5.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:12
Exact Mass:410.31445783
Heavy Atom Count:29
Complexity:428

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOC(=O)NC1CCC(CC1)CC2CCC(CC2)NC(=O)OCCCC

Technology Process of 4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine)

There total 6 articles about 4,4'-Methylenebis(N-butoxycarbonylcyclohexanamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 99305-42-7
dibutyl (methylene-bis(cyclohexane-4,1,diyl))dicarbamate

Guidance literature:: In acetonitrile; at 20 ℃; for 1h;

In acetonitrile; at 80 ℃; for 3h;

Reference yield: 94.0%

: 109-69-3
n-Butyl chloride

: 1761-71-3
4,4'-diaminodicyclohexylmethane

: 17351-61-0
tetraethylammonium bicarbonate

: 99305-42-7
dibutyl (methylene-bis(cyclohexane-4,1,diyl))dicarbamate

Guidance literature:: 4,4'-diaminodicyclohexylmethane; tetraethylammonium bicarbonate; In acetonitrile; at 20 ℃; for 1h; Green chemistry;

n-Butyl chloride; In acetonitrile; at 80 ℃; for 3h; Green chemistry;
DOI:10.1021/acs.oprd.8b00229

Reference yield: 88.0%

: 109-69-3
n-Butyl chloride

: 1761-71-3
4,4'-diaminodicyclohexylmethane

: 5-azoniaspiro[4.4]nonane hydrogen carbonate

: 99305-42-7
dibutyl (methylene-bis(cyclohexane-4,1,diyl))dicarbamate

Guidance literature:: 4,4'-diaminodicyclohexylmethane; 5-azoniaspiro[4.4]nonane hydrogen carbonate; In acetonitrile; at 20 ℃; for 1h; Green chemistry;

n-Butyl chloride; In acetonitrile; at 80 ℃; for 3h; Green chemistry;
DOI:10.1021/acs.oprd.8b00229