2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl

Base Information

• Chemical Name: 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl
• CAS No.: 74816-70-9
• Molecular Formula: C₁₇H₁₆N₄O₃
• Molecular Weight: 324.339

Synonyms:2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl

Chemical Property of 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl

Chemical Property:

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Technology Process of 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl

There total 5 articles about 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Benzalbis(N'-methylurea) + 5-(1,3-Dimethyl-2,4-dioxopyrimidil)methyl ketone (36980-95-7) → 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl (74816-70-9)

Guidance literature:

With hydrogenchloride; In butan-1-ol; for 8.5h; Heating;

DOI:10.1007/BF02401733

Reference yield: 22.0%

2,2',4-Trioxo-6'-phenyl-1,1',2,2',3,4-hexahydro-4',5-dipyrimidinyl (71167-21-0) + methyl iodide (74-88-4) → 2'-Methoxy-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl (74816-66-3) + 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl (74816-70-9) + 1,1',3'-Trimethyl-6-phenyl-1H,1'H-[4,5']bipyrimidinyl-2,2',4'-trione (74816-69-6)

Guidance literature:

With sodium methylate; In dimethyl sulfoxide; at 70 ℃; for 0.0833333h;

DOI:10.1007/BF02401733

Reference yield: 13.0%

2,2',4-Trioxo-6'-phenyl-1,1',2,2',3,4-hexahydro-4',5-dipyrimidinyl (71167-21-0) + dimethyl sulfate (77-78-1) → 2'-Methoxy-2,4-dioxo-1,3-dimethyl-6'-phenyl-1,2,3,4-tetrahydro-4',5-dipyrimidinyl (74816-66-3) + 2,2',4-Trioxo-1,3,3'-trimethyl-6'-phenyl-1,2,2',3,3',4-hexahydro-4',5-dipyrimidinyl (74816-70-9) + 1,1',3'-Trimethyl-6-phenyl-1H,1'H-[4,5']bipyrimidinyl-2,2',4'-trione (74816-69-6)

Guidance literature:

With sodium hydroxide; In water; for 4h;

DOI:10.1007/BF02401733

upstream raw materials:

2,2',4-Trioxo-6'-phenyl-1,1',2,2',3,4-hexahydro-4',5-dipyrimidinyl

dimethyl sulfate

5-(1,3-Dimethyl-2,4-dioxopyrimidil)methyl ketone

methyl iodide

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