C₄₈H₄₄N₂O₁₃

Base Information

Chemical Name:C₄₈H₄₄N₂O₁₃
CAS No.:1127247-00-0
Molecular Formula:C₄₈H₄₄N₂O₁₃
Molecular Weight:856.883
Hs Code.:

C<sub>48</sub>H<sub>44</sub>N<sub>2</sub>O<sub>13</sub>

Synonyms:C₄₈H₄₄N₂O₁₃

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Chemical Property of C₄₈H₄₄N₂O₁₃

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Technology Process of C₄₈H₄₄N₂O₁₃

There total 7 articles about C₄₈H₄₄N₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1127246-99-4
C₄₁H₄₁NO₉

: 7693-46-1
4-Nitrophenyl chloroformate

: 1127247-00-0
C₄₈H₄₄N₂O₁₃

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 1127247-00-0
C₄₈H₄₄N₂O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere

2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

4.1: sodium methylate / methanol / 12 h / 20 °C

4.2: Dowex_.(R). H⁺ resin / pH 5

5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.2: 12 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 12 h / 20 °C

With dmap; sodium tetrahydroborate; sodium methylate; sodium hydride; triethylamine; trifluoroacetic acid; silver(l) oxide; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;

Reference yield:

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 1127247-00-0
C₄₈H₄₄N₂O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere

2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

4.1: sodium methylate / methanol / 12 h / 20 °C

4.2: Dowex_.(R). H⁺ resin / pH 5

5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.2: 12 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 12 h / 20 °C

With dmap; sodium tetrahydroborate; sodium methylate; sodium hydride; triethylamine; trifluoroacetic acid; silver(l) oxide; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;