Technology Process of C18H15BrN2O2
There total 5 articles about C18H15BrN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethylene glycol;
at 245 ℃;
for 0.583333h;
Biotage Initiator microwave;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium tetrahydroborate; methanol / 2 h / 20 °C
2: triethylamine / dichloromethane / 20 °C
3: toluene-4-sulfonic acid; water / tetrahydrofuran / 4 h / 115 °C
4: ethanol / 1 h / 20 °C
5: diethylene glycol / 0.58 h / 245 °C / Biotage Initiator microwave
With
methanol; sodium tetrahydroborate; water; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; diethylene glycol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 20 °C
2: toluene-4-sulfonic acid; water / tetrahydrofuran / 4 h / 115 °C
3: ethanol / 1 h / 20 °C
4: diethylene glycol / 0.58 h / 245 °C / Biotage Initiator microwave
With
water; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; ethanol; dichloromethane; diethylene glycol;