(-)(R)-sec-butyl-acetamide

Base Information

• Chemical Name: (-)(R)-sec-butyl-acetamide
• CAS No.: 286414-05-9
• Molecular Formula: C₆H₁₃NO
• Molecular Weight: 115.175
• Mol file: 286414-05-9.mol

Synonyms:(-)(R)-sec-butyl-acetamide

Chemical Property of (-)(R)-sec-butyl-acetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)(R)-sec-butyl-acetamide

There total 3 articles about (-)(R)-sec-butyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

vinyl acetate (108-05-4,9003-20-7) + SEC-BUTYLAMINE (33966-50-6) → (S)-2-aminobutane (513-49-5) + (R)-sec-butylamine (13250-12-9) + (-)(R)-sec-butyl-acetamide (286414-05-9) + (S)-N-(sec-butyl)acetamide (1189-05-5,64528-59-2,64528-61-6)

Guidance literature:

With Aspergillus niger AC-54 lipase; In hexane; at 50 ℃; for 0.0166667h; under 2585.81 Torr; Microwave irradiation; Enzymatic reaction;

DOI:10.1590/S0103-50532012005000033

Reference yield:

Isopropenyl acetate (108-22-5) + SEC-BUTYLAMINE (33966-50-6) → (S)-2-aminobutane (513-49-5) + (R)-sec-butylamine (13250-12-9) + (-)(R)-sec-butyl-acetamide (286414-05-9) + (S)-N-(sec-butyl)acetamide (1189-05-5,64528-59-2,64528-61-6)

Guidance literature:

With Aspergillus niger AC-54 lipase; In hexane; at 50 ℃; for 0.0166667h; under 2585.81 Torr; Microwave irradiation; Enzymatic reaction;

DOI:10.1590/S0103-50532012005000033

Reference yield:

SEC-BUTYLAMINE (33966-50-6) + ethyl acetate (141-78-6) → (S)-2-aminobutane (513-49-5) + (R)-sec-butylamine (13250-12-9) + (-)(R)-sec-butyl-acetamide (286414-05-9) + (S)-N-(sec-butyl)acetamide (1189-05-5,64528-59-2,64528-61-6)

Guidance literature:

With Candida antarctica (Novozym 435); In diethyl ether; at 21 ℃; for 48h; Title compound not separated from byproducts; Enzymatic reaction;

DOI:10.1081/SCC-100000584

upstream raw materials:

SEC-BUTYLAMINE

ethyl acetate

vinyl acetate

Isopropenyl acetate