methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

Base Information

Chemical Name:methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate
CAS No.:1268830-95-0
Molecular Formula:C₂₀H₂₄FNO₆S
Molecular Weight:425.478
Hs Code.:

Synonyms:methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

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Chemical Property of methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

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Technology Process of methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

There total 5 articles about methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1268830-93-8
methyl 6-fluoro-2-methoxy-3-(propylsulfonamido)benzoate

: 824-94-2
p-methoxybenzyl chloride

: 1268830-95-0
methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

Guidance literature:: methyl 6-fluoro-2-methoxy-3-(propylsulfonamido)benzoate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Cooling with ice;

p-methoxybenzyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Cooling with ice;

Reference yield:

: 83141-10-0
2,6-difluoro-3-nitrobenzoic acid

: 1268830-95-0
methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / 2 h / Cooling with water bath

2.1: -4 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 60 h / 20 °C / 760.05 Torr / Inert atmosphere

4.1: dmap; pyridine / dichloromethane / 14.08 h / 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

5.2: 3 h / 20 °C / Cooling with ice

With pyridine; methanol; dmap; hydrogen; sodium hydride; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1268830-91-6
methyl 3-amino-6-fluoro-2-methoxybenzoate

: 1268830-95-0
methyl 6-fluoro-2-methoxy-3-(N-(4-methoxybenzyl)(propylsulfonamido))benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; pyridine / dichloromethane / 14.08 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

2.2: 3 h / 20 °C / Cooling with ice

With pyridine; dmap; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;