Technology Process of C33H50N4O7
There total 8 articles about C33H50N4O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 18h;
Cooling;
DOI:10.1021/jo4001492
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 0 - 20 °C
2: palladium 10% on activated carbon; hydrogen / acetic acid / 20 °C
3: triethylamine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 20 °C / Cooling
With
palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide;
In
acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo4001492
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 20 °C
2: lithium hydroxide / methanol; tetrahydrofuran; water / 2 h / 20 °C
3: triethylamine; benzotriazol-1-ol; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 18 h / 20 °C / Cooling
With
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo4001492