benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

Base Information

Chemical Name:benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate
CAS No.:1245904-41-9
Molecular Formula:C₂₃H₂₅NO₅
Molecular Weight:395.455
Hs Code.:

Synonyms:benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

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Chemical Property of benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

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Technology Process of benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

There total 1 articles about benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 5332-81-0,99260-79-4
carbonic acid (Z)-4-methoxycarbonyloxy-but-2-enyl ester methyl ester

: (E)-benzyl (1-phenylhexa-1,5-dien-3-yl)carbamate

: 1245904-41-9
benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; at 20 ℃; for 43h;
DOI:10.1021/ol101755m

Reference yield: 45.0%

: 1245904-41-9
benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate

: 4083-64-1
Tosyl isocyanate

: 1245904-46-4
benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-yl(tosylcarbamoyl)carbamate

Guidance literature:: benzyl (1E,5E)-7-(methoxycarbonyloxy)-1-phenylhepta-1,5-dien-3-ylcarbamate; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.25h;

Tosyl isocyanate; In diethyl ether; hexane; at -78 ℃; for 1.08333h;
DOI:10.1021/ol101755m