(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

Base Information

Chemical Name:(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate
CAS No.:1259282-27-3
Molecular Formula:C₃₁H₄₂O₇
Molecular Weight:526.67
Hs Code.:

Synonyms:(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

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Chemical Property of (1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

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Technology Process of (1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

There total 4 articles about (1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1259282-25-1
(1S,2S)-2-allyl-1-(3,4-dimethoxyphenyl)trimethylene dipivalate

: 5720-07-0
4-methoxyphenylboronic acid

: 1259282-27-3
(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

Guidance literature:: With lithium acetate; copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1271/bbb.100255

Reference yield: 30.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 1259282-25-1
(1S,2S)-2-allyl-1-(3,4-dimethoxyphenyl)trimethylene dipivalate

: 1259282-27-3
(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; triethylamine; In dichloromethane; at 40 ℃; for 9h;
DOI:10.1271/bbb.100255

Reference yield:

: 1259282-24-0
(1S,2S)-2-allyl-1-(3,4-dimethoxyphenyl)-1,3-propanediol

: 1259282-27-3
(1S,2S)-1-(3,4-dimethoxyphenyl)-2-[(E)-3-(4-methoxyphenyl)-2-propen-1-yl]trimethylene dipivalate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1 h / 20 °C

2: lithium acetate; copper diacetate; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C

With pyridine; lithium acetate; copper diacetate; palladium diacetate; In N,N-dimethyl-formamide; 2: Mizoroki-Heck reaction;
DOI:10.1271/bbb.100255