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C6H5Sn((2)H)3

Base Information
  • Chemical Name:C6H5Sn((2)H)3
  • CAS No.:354159-94-7
  • Molecular Formula:C6H8Sn
  • Molecular Weight:201.816
  • Hs Code.:
C<sub>6</sub>H<sub>5</sub>Sn(<sup>(2)</sup>H)3

Synonyms:C6H5Sn((2)H)3

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Chemical Property of C6H5Sn((2)H)3
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Technology Process of C6H5Sn((2)H)3

There total 1 articles about C6H5Sn((2)H)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In diethyl ether; a soln. of (C6H5)SnCl3 in (CH3CH2)2O was added dropwise to a soln. of LiAl((2)H)4 in (CH3CH2)2O which was cooled at -70°C, the resulting soln. was stirred for 30 min at -70°C and at -20°C for 60 min; the mixt. was filtered under N2, a filtrate was isolated and sepd. by distn., the volatiles were passed through traps held at -20°C and -196°C with retained (C6H5)Sn(2)H3 and (CH3CH2)2O;
DOI:10.1021/ja0115058
Guidance literature:
In neat (no solvent, gas phase); byproducts: benzene-d1; decompn. in an ultrahigh-vac. reactor at 250°C;
DOI:10.1021/ja0115058
upstream raw materials:

phenyltin trichloride

Downstream raw materials:

tin

deuterium

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