tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

Base Information

Chemical Name:tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid
CAS No.:1366179-34-1
Molecular Formula:C₁₂H₂₇N*C₁₄H₁₁ClO₃
Molecular Weight:448.046
Hs Code.:

Synonyms:tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

Suppliers and Price of tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

Chemical Property:

Purity/Quality:: 98% HPLC ^*data from raw suppliers

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Technology Process of tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

There total 2 articles about tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-82-9
tributyl-amine

: 57486-68-7
methyl (2-chlorophenyl)acetate

: 106-48-9,82344-39-6
4-chloro-phenol

: 1366179-34-1
tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

Guidance literature:: methyl (2-chlorophenyl)acetate; 4-chloro-phenol; With caesium carbonate; dimethylaminoacetic acid; copper(l) chloride; In 1,4-dioxane; at 110 - 115 ℃;

With potassium hydroxide; In methanol; at 25 - 65 ℃; for 5h;

tributyl-amine;

Reference yield:

: 2444-36-2
2'-chloro-benzeneacetic acid

: 1366179-34-1
tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 1 h / Reflux

2.1: caesium carbonate / copper(l) chloride; dimethylaminoacetic acid / 1,4-dioxane / 110 - 115 °C

2.2: 5 h / 25 - 65 °C

With caesium carbonate; dimethylaminoacetic acid; sulfuric acid; copper(l) chloride; In 1,4-dioxane;

Reference yield:

: 1366179-34-1
tributylamine salt of 2-(2-(4-chlorophenoxy)phenyl)acetic acid

: 65576-45-6,65621-78-5
asenapine

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / dichloromethane; water / pH 1.5

1.2: 0.75 h / 0 - 15 °C

2.1: potassium tert-butylate / toluene / 3 h / 20 °C

2.2: 3 h / 20 °C

3.1: phosphorus pentoxide; phosphoric acid / 96 h / 115 - 120 °C

4.1: formic acid; iodine; magnesium / toluene; methanol / 5 h / 20 - 40 °C

4.2: 5 - 10 °C / pH ~ 1

5.1: sodium tetrahydroborate / tetrahydrofuran / 0.25 h / 20 °C

5.2: 6 h / Reflux

5.3: 10 - 15 °C

With hydrogenchloride; sodium tetrahydroborate; formic acid; phosphorus pentoxide; phosphoric acid; potassium tert-butylate; iodine; magnesium; In tetrahydrofuran; methanol; dichloromethane; water; toluene;