tetra(trimethylsilyl) dimethylaminomethylenediphosphonate

Base Information

• Chemical Name: tetra(trimethylsilyl) dimethylaminomethylenediphosphonate
• CAS No.: 106753-26-8
• Molecular Formula: C₁₅H₄₃NO₆P₂Si₄
• Molecular Weight: 507.799
• Mol file: 106753-26-8.mol

Synonyms:tetra(trimethylsilyl) dimethylaminomethylenediphosphonate

Chemical Property of tetra(trimethylsilyl) dimethylaminomethylenediphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tetra(trimethylsilyl) dimethylaminomethylenediphosphonate

There total 1 articles about tetra(trimethylsilyl) dimethylaminomethylenediphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

tris(trimethylsilyl) phosphite (1795-31-9) + ethyl formimidate hydrochloride (16694-46-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → tetra(trimethylsilyl) dimethylaminomethylenediphosphonate (106753-26-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1134/S1070363215020048

Reference yield: 97.0%

tetra(trimethylsilyl) dimethylaminomethylenediphosphonate (106753-26-8) → (dimethylaminomethylene)diphosphonic acid (29712-30-9)

Guidance literature:

With methanol; at 10 ℃; Reflux; Inert atmosphere;

DOI:10.1002/hc.21100

upstream raw materials:

tris(trimethylsilyl) phosphite

ethyl formimidate hydrochloride

N,N-dimethyl-formamide

Downstream raw materials:

(dimethylaminomethylene)diphosphonic acid