C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

Base Information

Chemical Name:C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2
CAS No.:1020853-36-4
Molecular Formula:C₃₁H₆₀Ga₂Si
Molecular Weight:600.349
Hs Code.:

C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>C(Si(CH<sub>3</sub>)3)(Ga(CH<sub>2</sub>C(CH<sub>3</sub>)3)2)2

Synonyms:C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

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Chemical Property of C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

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Technology Process of C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

There total 1 articles about C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1005391-33-2
[C₆H₅CH₂C(Si(CH₃)3)(GaCl₂)2]2

: 7412-67-1
neopentyl lithium

: 1020853-36-4
C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

Guidance literature:: In toluene; byproducts: LiCl; (Ar); Ga compd. was dissolved in toluene at 50 to 60°C; cooled to-80°C; soln. of Li compd. (4 equiv.) in toluene was added dropwi se; warmed to room temp.; stirred for 24 h; concd. (vac.); filtered; concd.; cooled to -45°C; elem. anal.;
DOI:10.1021/om800068s

Reference yield: 72.0%

: 1020853-36-4
C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

: 4670-62-6
tetra-N-butylammonium benzenethiolate

: 1020853-38-6
(C₄H₉)4N⁽¹⁺⁾*[C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2SC₆H₅]^(1-)=[(C₄H₉)4N][C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2SC₆H₅]

Guidance literature:: In further solvent(s); (Ar); mixt. of thiophenolate in 1,2-difluorobenzene was added dropwise to Ga compd. in 1,2-difluorobenzene at room temp.; stirred for 3 h; concd.; cooled to 4°C; elem. anal.;
DOI:10.1021/om800068s

Reference yield: 50.0%

: 1020853-36-4
C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2

: 18819-89-1
tetrabutylammonium benzoate

: 1020853-40-0
(C₄H₉)4N⁽¹⁺⁾*C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2O₂CC₆H₅^(1-)=(C₄H₉)4N[C₆H₅CH₂C(Si(CH₃)3)(Ga(CH₂C(CH₃)3)2)2O₂CC₆H₅]

Guidance literature:: In toluene; (Ar); soln. of benzoate in toluene was added dropwise to Ga compd. in toluene at room temp.; stirred for 4 h; filtered; concd.; cooled to -45°C; oily phase septd.; dissolved in 1,2-difluorobenzene; cooled to -4°C; elem. anal.;
DOI:10.1021/om800068s