4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

Base Information

Chemical Name:4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid
CAS No.:91540-81-7
Molecular Formula:C₂₄H₂₈O₆S
Molecular Weight:444.549
Hs Code.:

Synonyms:4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

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Chemical Property of 4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

Chemical Property:

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Technology Process of 4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

There total 6 articles about 4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91541-92-3
4-{4-[3-(4-Acetyl-3-hydroxy-2-propyl-phenoxy)-propylsulfanyl]-phenyl}-4-oxo-butyric acid methyl ester

: 91540-81-7
4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jm00159a003

Reference yield:

: 56872-39-0
3-(4-hydroxybenzoyl)propionic acid

: 91540-81-7
4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / dimethylformamide

2: 2.) NaOMe / 1.) 200 deg C, 2.) MeOH

3: K₂CO₃ / butan-2-one / 4 h / Heating

4: NaOH / methanol; tetrahydrofuran

With sodium hydroxide; sodium methylate; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; butanone;
DOI:10.1021/jm00159a003

Reference yield:

: 100-66-3
methoxybenzene

: 91540-81-7
4-((3-(4-Acetyl-3-hydroxy-2-propylphenoxy)propyl)thio)-gamma-oxobenzenebutanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: AlCl₃ / 1,2-dichloro-ethane / 0 °C

2: HBr, HOAc / Heating

3: NaH / dimethylformamide

4: 2.) NaOMe / 1.) 200 deg C, 2.) MeOH

5: K₂CO₃ / butan-2-one / 4 h / Heating

6: NaOH / methanol; tetrahydrofuran

With sodium hydroxide; aluminium trichloride; hydrogen bromide; sodium methylate; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; butanone;
DOI:10.1021/jm00159a003