thallous salt of N-methylsalicylaldimine

Base Information

Chemical Name:thallous salt of N-methylsalicylaldimine
CAS No.:432050-08-3
Molecular Formula:C₈H₈NOTl
Molecular Weight:338.541
Hs Code.:

Synonyms:thallous salt of N-methylsalicylaldimine

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Chemical Property of thallous salt of N-methylsalicylaldimine

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Technology Process of thallous salt of N-methylsalicylaldimine

There total 1 articles about thallous salt of N-methylsalicylaldimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 3117-65-5
2-(methyliminomethyl)phenol

: 20398-06-5
thallium (I) ethoxide

: 432050-08-3
thallous salt of N-methylsalicylaldimine

Guidance literature:: In tetrahydrofuran; (Ar), mixed dropwise at room temp., stirred at room temp. for 2 h; filtered (N2);
DOI:10.1016/S1381-1169(01)00451-4

Reference yield: 78.0%

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 432050-08-3
thallous salt of N-methylsalicylaldimine

: 1600523-84-9
C₄₄H₃₈ClNOP₂Ru

Guidance literature:: In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.molcata.2014.02.009

Reference yield: 77.0%

: trans-chloro-1,4-bis(p-methoxyphenyl)-1,4-diaza-3-methylbutadiene-2-yl-bis(triphenylphosphine)palladium(II)

: 432050-08-3
thallous salt of N-methylsalicylaldimine

: [Pd(N-methylsalicylaldiminato)(C(N-p-C₆H₄OMe)CMe=N-p-C₆H₄OMe)(PPh₃)]

Guidance literature:: In benzene; soln. of Pd-complex in benzene reacted with Tl salt (molar ratio 1:1.5), stirred for 6 h in the dark; treated with charcoal, filtered, concd., pptd. with n-pentane, purifiedby two re-pptns. from benzene-n-pentane; elem. anal.;
DOI:10.1016/S0020-1693(00)90850-8