Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate

Base Information

• Chemical Name: Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate
• CAS No.: 118509-96-9
• Molecular Formula: C₁₂H₁₃NO₆
• Molecular Weight: 267.238
• Hs Code.: 2916120090
• Mol file: 118509-96-9.mol

Synonyms:(E)-3-(4,5-dimethoxy-2-nitro-phenyl)-acrylic acid methyl ester

Chemical Property of Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate

There total 4 articles about Methyl 3-(4,5-dimethoxy-2-nitrophenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

6-nitroveratraldehyde (20357-25-9) + methyl (triphenylphosphoranylidene)acetate (21204-67-1,2605-67-6) → (E)-3-(4,5-dimethoxy-2-nitro-phenyl)-acrylic acid methyl ester (118509-96-9)

Guidance literature:

In toluene; for 3h; Reflux;

Reference yield:

6-nitroveratraldehyde (20357-25-9) → (E)-3-(4,5-dimethoxy-2-nitro-phenyl)-acrylic acid methyl ester (118509-96-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; piperidine

2: hydrogen chloride

With piperidine; pyridine; hydrogenchloride;

Reference yield:

methanol (67-56-1) + 6-nitro-3,4-dimethoxycinnamic acid (20567-38-8) → (E)-3-(4,5-dimethoxy-2-nitro-phenyl)-acrylic acid methyl ester (118509-96-9)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

methanol

6-nitro-3,4-dimethoxycinnamic acid

6-nitroveratraldehyde

methyl (triphenylphosphoranylidene)acetate

Downstream raw materials:

6,7-dimethoxy-3,4-dihydroquinolin-2(1H)-one

3-(2-amino-4,5-dimethoxyphenyl)acrylic acid methyl ester

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