Chloronitroacetyl chloride

Base Information

• Chemical Name: Chloronitroacetyl chloride
• CAS No.: 85915-53-3
• Molecular Formula: C₂HCl₂NO₃
• Molecular Weight: 157.941
• Mol file: 85915-53-3.mol

Synonyms:Chloronitroacetyl chloride

Chemical Property of Chloronitroacetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Chloronitroacetyl chloride

There total 1 articles about Chloronitroacetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Trichloroethylene (79-01-6) → dichloroacethyl chloride (79-36-7) + pentachloroethane (76-01-7) + Chloronitroacetyl chloride (85915-53-3)

Guidance literature:

With sulfuric acid; nitric acid; at 14 - 16 ℃; for 0.5h; Product distribution; dependence on the HNO₃ content and on the H₂SO₄ content in the nitration mixture and on the amount of this mixture;

Reference yield: 75.0%

Chloronitroacetyl chloride (85915-53-3) → dichloroformoxime (1794-86-1)

Guidance literature:

With urea; In diethyl ether; for 0.5h; Heating; further reagents (C₆H₁₁NH)2CO, (MeNH)2CO, thiourea, (PhNH)2CO;

DOI:10.1007/BF00954248

Reference yield: 68.0%

Chloronitroacetyl chloride (85915-53-3) + toluene (108-88-3,15644-74-3,16713-13-6) → p-Toluic acid (99-94-5)

Guidance literature:

With aluminium trichloride; for 2h;

DOI:10.1007/BF00953106

upstream raw materials:

Trichloroethylene

Downstream raw materials:

(chloro-nitro-methylene)-phenyl-hydrazine

dichloroformoxime

monochloronitromethane

3-chloro-5-phenylisoxazole