methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

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Chemical Name:methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate
CAS No.:1197029-49-4
Molecular Formula:C₃₇H₃₄Br₂O₈
Molecular Weight:766.48
Hs Code.:

Synonyms:methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

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Chemical Property of methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

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Technology Process of methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

There total 4 articles about methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 20769-85-1
2-bromoisobutyric acid bromide

: 1197029-47-2
methyl 6-hydroxy-2-(4-(2-hydroxyethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

: 1197029-49-4
methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1021/ma901830b

Reference yield:

: 869796-85-0
1-(4-(2-hydroxyethoxy)phenyl)-1-phenylprop-2-yn-1-ol

: 1197029-49-4
methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With triethylamine; In dichloromethane;
DOI:10.1021/ma901830b

Reference yield:

: 14814-17-6
(4-(2-hydroxyethoxy)phenyl)(phenyl)methanone

: 1197029-49-4
methyl 6-(2-bromo-2-methylpropanoyloxy)-2-(4-(2-(2-bromo-2-methylpropanoyloxy)ethoxy)phenyl)-2-phenyl-2H-naphtho[1,2-b]pyran-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / hexane

3: triethylamine / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice

With n-butyllithium; triethylamine; In hexane; dichloromethane;
DOI:10.1021/ma901830b