tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate

Base Information

Chemical Name:tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate
CAS No.:188422-36-8
Molecular Formula:CF₃O₃S*C₅₄H₄₅Au₃OP₃
Molecular Weight:1542.84
Hs Code.:

Synonyms:tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate

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Technology Process of tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate

There total 3 articles about tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 2923-28-6
silver trifluoromethanesulfonate

: 188422-36-8
C₅₄H₄₅Au₃OP₃⁽¹⁺⁾*CF₃O₃S^(1-)

Guidance literature:: In tetrahydrofuran; for 0.0833333h; Darkness;
DOI:10.1002/chem.201201215

Reference yield: 31.0%

: 3-[(triphenylphosphine)gold]pentane-2,4-dione

: 7732-18-5
water

: 60933-18-8
diethylammonium trifluoromethanesulfonate

: 188422-36-8
tris[(triphenylphosphine)gold(I)]oxonium trifluoromethanesulfonate

Guidance literature:: In acetone; byproducts: Au; dropwise addn. of ammonium salt to Au-complex, stirring at room temp. for 10 h (source of water unclear); filtration over MgSO4, concn., pptn. on Et2O addn., collection (filtration), washing (Et2O), drying in air; elem. anal.;
DOI:10.1021/ic970225j