N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine

Base Information

• Chemical Name: N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine
• CAS No.: 1427036-71-2
• Molecular Formula: C₂₉H₃₆BNO₂
• Molecular Weight: 441.421

Synonyms:N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine

Chemical Property of N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine

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Technology Process of N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine

There total 2 articles about N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-propenylbenzene (873-66-5) + N,N-dibenzyl-O-benzoylhydroxylamine (52742-32-2) + bis(pinacol)diborane (73183-34-3) → N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine (1427036-71-2)

Guidance literature:

With 1,2-bis((2S,5S)-2,5-dimethylphospholano)benzene; copper(l) chloride; lithium tert-butoxide; In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1021/ja4007645

Reference yield:

1-propenylbenzene (873-66-5) + N,N-dibenzyl-O-benzoylhydroxylamine (52742-32-2) + bis(pinacol)diborane (73183-34-3) → N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine (1427036-71-2) + (1S,2R)-N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine

Guidance literature:

With C₃₂H₄₆N₂O₂P₂; copper(I) bromide; lithium tert-butoxide; In tetrahydrofuran; at 23 ℃; for 16h; Reagent/catalyst; Overall yield = 49 percent; enantioselective reaction; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.9b03328

Reference yield:

N,N-dibenzyl-1-phenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propan-1-amine (1427036-71-2) → C23H25NO (1427036-67-6)

Guidance literature:

With sodium perborate tetrahydrate; In tetrahydrofuran; water;

DOI:10.1021/ja4007645

upstream raw materials:

1-propenylbenzene

N,N-dibenzyl-O-benzoylhydroxylamine

bis(pinacol)diborane

Downstream raw materials:

C₂₃H₂₅NO

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