1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

Base Information

Chemical Name:1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate
CAS No.:1215106-26-5
Molecular Formula:C₉H₁₁O₃S*C₂₄H₂₉N₄O₄S
Molecular Weight:668.835
Hs Code.:

Synonyms:1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

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Chemical Property of 1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

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Technology Process of 1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

There total 10 articles about 1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1215106-23-2
3-(3-(N-(2-(tert-butyldimethylsilyloxy)ethyl)methylsulfonamido)pyridin-4-yl)-N-(2-phenylpropan-2-yl)benzamide

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 1215106-26-5
1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 25487-66-5
3-Carboxyphenylboronic acid

: 1215106-26-5
1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / HATU / N,N-dimethyl-formamide / 1 h / 20 °C

3: hydrogen / palladium 10% on activated carbon / water; methanol / 2 h

4: triethylamine / dichloromethane / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 60 °C

6: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

7: dichloromethane / 0 - 20 °C

With tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; HATU; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 13091-23-1
4-chloro-3-nitropyridine

: 1215106-26-5
1-amino-3-(N-(2-hydroxyethyl)methylsulfonamido)-4-(3-(2-phenylpropan-2-ylcarbamoyl)phenyl)pyridinium 2,4,6-trimethylbenzenesulfonate

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 15 h / 100 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / HATU / N,N-dimethyl-formamide / 1 h / 20 °C

3: hydrogen / palladium 10% on activated carbon / water; methanol / 2 h

4: triethylamine / dichloromethane / 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 60 °C

6: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C

7: dichloromethane / 0 - 20 °C

With tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; HATU; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;