C₁₇H₂₄O₂SeSi

Base Information

Chemical Name:C₁₇H₂₄O₂SeSi
CAS No.:1416429-78-1
Molecular Formula:C₁₇H₂₄O₂SeSi
Molecular Weight:367.422
Hs Code.:

C<sub>17</sub>H<sub>24</sub>O<sub>2</sub>SeSi

Synonyms:C₁₇H₂₄O₂SeSi

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Chemical Property of C₁₇H₂₄O₂SeSi

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Technology Process of C₁₇H₂₄O₂SeSi

There total 6 articles about C₁₇H₂₄O₂SeSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 5707-04-0
Phenylselenyl chloride

: 56745-67-6,61305-35-9,61740-33-8,61305-36-0
(4S)-4-tert-butyldimethylsilyloxycyclopent-2-en-1-one

: 1416429-78-1
C₁₇H₂₄O₂SeSi

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol303071t

Reference yield:

: 98-00-0,25212-86-6,93793-62-5
(2-furyl)methyl alcohol

: 1416429-78-1
C₁₇H₂₄O₂SeSi

Guidance literature:: Multi-step reaction with 6 steps

1: potassium dihydrogenphosphate / water / 48 h / Inert atmosphere; Reflux

2: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

3: lithium aluminium tetrahydride; lithium iodide / diethyl ether / -45 - -40 °C / Inert atmosphere

4: triethylamine; Pancreatin; vinyl acetate / tert-butyl methyl ether / 8 h / 20 °C / Inert atmosphere; Sealed tube; Enzymatic reaction

5: pyridinium chlorochromate; sodium acetate / dichloromethane / 1.08 h / 20 °C / Inert atmosphere

6: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; Pancreatin; potassium dihydrogenphosphate; lithium aluminium tetrahydride; vinyl acetate; sodium acetate; triethylamine; pyridinium chlorochromate; lithium iodide; In diethyl ether; dichloromethane; tert-butyl methyl ether; water;
DOI:10.1021/ol303071t

Reference yield:

: 59995-47-0,59995-49-2,61305-27-9,61740-29-2
4-Hydroxycyclopent-2-enone

: 1416429-78-1
C₁₇H₂₄O₂SeSi

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride; lithium iodide / diethyl ether / -45 - -40 °C / Inert atmosphere

3: triethylamine; Pancreatin; vinyl acetate / tert-butyl methyl ether / 8 h / 20 °C / Inert atmosphere; Sealed tube; Enzymatic reaction

4: pyridinium chlorochromate; sodium acetate / dichloromethane / 1.08 h / 20 °C / Inert atmosphere

5: pyridine / dichloromethane / 20 °C / Inert atmosphere

With pyridine; dmap; Pancreatin; lithium aluminium tetrahydride; vinyl acetate; sodium acetate; triethylamine; pyridinium chlorochromate; lithium iodide; In diethyl ether; dichloromethane; tert-butyl methyl ether;
DOI:10.1021/ol303071t