1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

Base Information

Chemical Name:1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one
CAS No.:69282-90-2
Molecular Formula:C₂₉H₂₈N₂O₅
Molecular Weight:484.552
Hs Code.:

1-[<i>O</i><sup>5</sup>-(4-methoxy-trityl)-β-<i>D</i>-<i>erythro</i>-2-deoxy-pentofuranosyl]-1<i>H</i>-pyrimidin-2-one

Synonyms:1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

Suppliers and Price of 1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

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Chemical Property of 1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

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Technology Process of 1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

There total 1 articles about 1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69282-90-2
1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

Guidance literature:: Nucleosid 2, Monomethoxy-tritylchlorid;
DOI:10.1002/hlca.19780610728

Reference yield: 88.0%

: 93-97-0
benzoic acid anhydride

: 69282-90-2
1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

: 86359-80-0
Benzoic acid (2R,3S,5R)-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-(2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: With dmap; In pyridine; for 3h;
DOI:10.1002/hlca.19830660131

Reference yield:

: 69282-90-2
1-[O⁵-(4-methoxy-trityl)-β-D-erythro-2-deoxy-pentofuranosyl]-1H-pyrimidin-2-one

: 86359-81-1
Benzoic acid (2R,3S,5R)-2-hydroxymethyl-5-(2-oxo-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 4-dimethylaminopyridine / pyridine / 3 h

2: 89.5 percent / 2percent benzenesulfonic acid / CHCl₃; methanol / 0.67 h

With dmap; benzenesulfonic acid; In pyridine; methanol; chloroform;
DOI:10.1002/hlca.19830660131