Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

Base Information

• Chemical Name: Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2
• CAS No.: 87101-15-3
• Molecular Formula: C₇₄H₆₅N₃P₄Pt₂*2ClO₄
• Molecular Weight: 1709.31

Synonyms:Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

Chemical Property of Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

Chemical Property:

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Technology Process of Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

There total 2 articles about Pt₂(CH₃C₆H₄NC)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)3((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

dichlorobis(bis(diphenylphosphino)methane)dichloroplatinum(I) (61250-65-5) + 4-methylphenyl isocyanide (7175-47-5) + sodium perchlorate → Pt2(CH3C6H4NC)(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2(2+)*2ClO4(1-)=(Pt2(CH3C6H4NC)3((C6H5)2PCH2P(C6H5)2)2)(ClO4)2 (87101-15-3)

Guidance literature:

In methanol; byproducts: NaCl; under N2, to Pt2Cl2(dppm)2 was added a soln. of NaClO4 in methanol followed by a soln. of MeC6H4NC (molar ratio 1:6:4), stirred; filtered, evapd., extd. with CH2Cl2, filtered, added EtOH, evapd., recrystd. from CH2Cl2-EtOH, vac. dried at 100.degreee.C; elem. anal.;

DOI:10.1021/om50006a006

Reference yield:

Pt2(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2(2+)*2ClO4(1-)=(Pt2(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2)(ClO4)2 (87101-13-1) + 4-methylphenyl isocyanide (7175-47-5) → Pt2(CH3C6H4NC)(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2(2+)*2ClO4(1-)=(Pt2(CH3C6H4NC)3((C6H5)2PCH2P(C6H5)2)2)(ClO4)2 (87101-15-3)

Guidance literature:

In not given; under N2, excess of isocyanide was added to soln. of Pt-complex;

DOI:10.1021/om50006a006

Reference yield: 94.0%

Pt2(CH3C6H4NC)(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2(2+)*2ClO4(1-)=(Pt2(CH3C6H4NC)3((C6H5)2PCH2P(C6H5)2)2)(ClO4)2 (87101-15-3) → Pt2(CH3C6H4N(H)C)(CH3C6H4NC)2((C6H5)2PCH2P(C6H5)2)2(3+)*3ClO4(1-)=(Pt2(CNHC6H4CH3)(CH3C6H4NC)2(C25H22P2)2)(ClO4)3 (87114-16-7)

Guidance literature:

With HClO₄; In ethanol; dichloromethane; under N2, to a soln. of Pt2(μ-CNC6H4CH3)(CNC6H4CH3)2(dppm)2(ClO4)2 in CH2Cl2-EtOH is added 70% HClO4; solvent removed, filtered, washed with acidified EtOH, recrystd. from CH2Cl2-acidified EtOH, filtered, washed with Et2O, vac. dried at 100°C; elem. anal.;

DOI:10.1021/om50006a006

upstream raw materials:

dichlorobis(bis(diphenylphosphino)methane)dichloroplatinum(I)

4-methylphenyl isocyanide

Pt₂(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

Downstream raw materials:

Pt₂(CH₃C₆H₄N(CH₃)C)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽³⁺⁾*3ClO₄^(1-)=(Pt₂(CN(CH₃)C₆H₄CH₃)(CH₃C₆H₄NC)2(C₂₅H₂₂P₂)2)(ClO₄)3

Pt₂(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽²⁺⁾*2ClO₄^(1-)=(Pt₂(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2)(ClO₄)2

Pt₂(CH₃C₆H₄N(H)C)(CH₃C₆H₄NC)2((C₆H₅)2PCH₂P(C₆H₅)2)2⁽³⁺⁾*3ClO₄^(1-)=(Pt₂(CNHC₆H₄CH₃)(CH₃C₆H₄NC)2(C₂₅H₂₂P₂)2)(ClO₄)3

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