N-benzyl-1-cyclopropyl methanimine

Base Information

• Chemical Name: N-benzyl-1-cyclopropyl methanimine
• CAS No.: 275800-36-7
• Molecular Formula: C₁₁H₁₃N
• Molecular Weight: 159.231
• Mol file: 275800-36-7.mol

Synonyms:N-benzyl-1-cyclopropyl methanimine

Chemical Property of N-benzyl-1-cyclopropyl methanimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-benzyl-1-cyclopropyl methanimine

There total 1 articles about N-benzyl-1-cyclopropyl methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzylamine (100-46-9) + Cyclopropanecarboxaldehyde (1489-69-6) → N-benzyl-1-cyclopropyl methanimine (275800-36-7)

Guidance literature:

With magnesium sulfate; In dichloromethane; at 20 ℃; for 48h;

Reference yield: 53.0%

carbon monoxide (201230-82-2) + 2-iodophenylamine (615-43-0) + N-benzyl-1-cyclopropyl methanimine (275800-36-7) → 3-benzyl-2-cyclopropyl-2,3-dihydroquinazolin-4(1H)-one

Guidance literature:

With potassium phosphate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; at 120 ℃; for 12h; under 760.051 Torr; Inert atmosphere; Schlenk technique;

DOI:10.1002/asia.202000359

Reference yield: 41.0%

(trifluoromethyl)trimethylsilane (81290-20-2) + N-benzyl-1-cyclopropyl methanimine (275800-36-7) → N-benzyl-1-cyclopropyl-2,2,2-trifluoroethan-1-amine

Guidance literature:

N-benzyl-1-cyclopropyl methanimine; With potassium hydrogenfluoride; trifluoroacetic acid; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃;

(trifluoromethyl)trimethylsilane; In N,N-dimethyl-formamide; acetonitrile; at 0 - 20 ℃; for 12h;

upstream raw materials:

benzylamine

Cyclopropanecarboxaldehyde