di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

Base Information

Chemical Name:di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate
CAS No.:1446011-80-8
Molecular Formula:C₂₆H₃₈N₈O₆S
Molecular Weight:590.704
Hs Code.:

Synonyms:di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

There total 2 articles about di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 6367-36-8
tert-butyl 2-azidoacetate

: 1446011-78-4
4-(2-(di(prop-2-yn-1-yl)amino)ethyl)benzenesulfonamide

: 1446011-80-8
di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

Guidance literature:: With copper; copper(II) sulfate; In tetrahydrofuran; water; at 20 ℃;

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1446011-80-8
di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile; toluene / 20 °C

2: copper; copper(II) sulfate / tetrahydrofuran; water / 20 °C

With copper; copper(II) sulfate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; toluene; acetonitrile;

Reference yield: 90.0%

: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]

: 1446011-80-8
di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate

: 1446011-62-6
C₂₁H₂₂N₈O₉ReS⁽¹⁺⁾

Guidance literature:: (NEt₄)2[rhenium(I)(bromide)3(carbonyl)3]; di-tert-butyl 2,2'-(4,4'-(((4-sulfamoylphenethyl)azanediyl)bis(methylene))bis(1H-1,2,3-triazole-4,1-diyl))diacetate; In acetonitrile; at 95 ℃; for 2h; Inert atmosphere; Autoclave;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;