4.5-DICHLORO-4,5,5-TRIFLUORO-1-PENTANOL

Base Information

• Chemical Name: 4.5-DICHLORO-4,5,5-TRIFLUORO-1-PENTANOL
• CAS No.: 97915-27-0
• Molecular Formula: C₅H₇Cl₂F₃O
• Molecular Weight: 211.011
• Mol file: 97915-27-0.mol

Synonyms:4,5-Dichloro-4,5,5-trifluoro-1-pentanol

Chemical Property of 4.5-DICHLORO-4,5,5-TRIFLUORO-1-PENTANOL

Chemical Property:

• Boiling Point: 82-83°C 7mm

Purity/Quality:

99%min. ^*data from raw suppliers

4,5-Dichloro-4,5,5-trifluoropentan-1-ol 97% ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

Useful:

Technology Process of 4.5-DICHLORO-4,5,5-TRIFLUORO-1-PENTANOL

There total 2 articles about 4.5-DICHLORO-4,5,5-TRIFLUORO-1-PENTANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

2-Iodo-4,5,5-trifluoro-4,5-dichloropentanol (1869-18-7) → 4,5-Dichloro-4,5,5-trifluoro pentanol (97915-27-0)

Guidance literature:

With tri-n-butyl-tin hydride; for 3h; Ambient temperature;

DOI:10.1016/S0022-1139(98)00251-6

Reference yield: 48.0%

1,1,2-Trichloro-1,2,2-trifluoroethane (76-13-1) + allyl alcohol (107-18-6) → 4,5-Dichloro-4,5,5-trifluoro pentanol (97915-27-0)

Guidance literature:

With sodium dithionite; water; sodium hydrogencarbonate; In acetonitrile; at 40 - 45 ℃; for 20h;

DOI:10.1016/S0022-1139(98)00246-2

Reference yield: 70.0%

4,5-Dichloro-4,5,5-trifluoro pentanol (97915-27-0) → 4,5,5-trifluoro-4-ene-pentanol (109993-33-1)

Guidance literature:

With acetic anhydride; acetic acid; zinc; at 90 ℃; for 4h;

DOI:10.1016/S0022-1139(98)00251-6

upstream raw materials:

2-Iodo-4,5,5-trifluoro-4,5-dichloropentanol

1,1,2-Trichloro-1,2,2-trifluoroethane

allyl alcohol

Downstream raw materials:

4,5,5-trifluoro-4-ene-pentanol