phenylazo-i-butyric acid nitrile

Base Information

• Chemical Name: phenylazo-i-butyric acid nitrile
• CAS No.: 1825-33-8
• Molecular Formula: C₁₀H₁₁N₃
• Molecular Weight: 173.217
• Mol file: 1825-33-8.mol

Synonyms:phenylazo-i-butyric acid nitrile

Chemical Property of phenylazo-i-butyric acid nitrile

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of phenylazo-i-butyric acid nitrile

There total 2 articles about phenylazo-i-butyric acid nitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

sodium cyanide (143-33-9,25596-52-5) + acetone phenylhydrazone (103-02-6) → phenylazo-i-butyric acid nitrile (1825-33-8)

Guidance literature:

With acetic acid; potassium iodide; In methanol; at 15 ℃; Electrochemical reaction;

DOI:10.1055/s-2003-41048

Reference yield:

α-(N'-phenyl-hydrazino)-isobutyronitrile (52722-61-9) → phenylazo-i-butyric acid nitrile (1825-33-8)

Guidance literature:

With chloroform; bromine; potassium bromide;

DOI:10.1039/jr9580001297

Reference yield:

tris(2,2,2-trifluoroethyl)phosphite (370-69-4) + bis(4-tert-butylphenyl)iodonium hexafluorophosphate (61358-25-6) + phenylazo-i-butyric acid nitrile (1825-33-8) → tris(2,2,2-trifluoroethyl) phosphate (358-63-4) + 1-tert-butyl-4-iodobenzene (35779-04-5) + bis(2,2,2-trifluoroethyl) tert-butylphenylphosphonate (1428647-08-8) + Phenyl-phosphonic acid bis-(2,2,2-trifluoro-ethyl) ester (172422-37-6)

Guidance literature:

With cyclohexane-1,2-epoxide; In neat (no solvent); at 34 ℃; for 4.16667h; UV-irradiation;

DOI:10.1021/jo302830r

upstream raw materials:

α-(N'-phenyl-hydrazino)-isobutyronitrile

sodium cyanide

acetone phenylhydrazone

Downstream raw materials:

α-phenylazo-isobutyric acid amide

iodobenzene

2-iodo-2-methylpropanenitrile

2,2,3,3-tetramethylsuccinonitrile