3-(Phenylthio)propionamide

Base Information

Chemical Name:3-(Phenylthio)propionamide
CAS No.:97721-47-6
Molecular Formula:C9H11 N O S
Molecular Weight:181.258
Hs Code.:2930909090
DSSTox Substance ID:DTXSID70469685
Nikkaji Number:J1.003.238E
Wikidata:Q82297507
Mol file:97721-47-6.mol

Synonyms:3-(PHENYLTHIO)PROPIONAMIDE;97721-47-6;SCHEMBL953807;DTXSID70469685;AKOS005233949;Z33547211

Suppliers and Price of 3-(Phenylthio)propionamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-(Phenylthio)propionamide

Chemical Property:

PSA：68.39000
LogP:2.35440
XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:181.05613515
Heavy Atom Count:12
Complexity:144

Purity/Quality:: 96% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SCCC(=O)N

Technology Process of 3-(Phenylthio)propionamide

There total 6 articles about 3-(Phenylthio)propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-98-5
thiophenol

: 79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5
2-propenamide

: 97721-47-6
3-(phenylsulfanyl)propanamide

Guidance literature:: With nickel(II) ferrite; In water; Green chemistry;
DOI:10.1039/c6ra21160g

Reference yield:

: 51849-21-9
β-(phenylthio)propionyl chloride

: 97721-47-6
3-(phenylsulfanyl)propanamide

Guidance literature:: With ammonium hydroxide; at 0 ℃; for 1h; Yield given;
DOI:10.1248/cpb.39.2225

Reference yield:

: 22198-59-0
methyl 3-phenylthiopropanoate

: 97721-47-6
3-(phenylsulfanyl)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / aq. KOH / ethanol / 1 h / Heating

2: DMF, SOCl₂ / 1 h / Heating

3: 28percent aq. NH₄OH / 1 h / 0 °C

With potassium hydroxide; ammonium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In ethanol;
DOI:10.1248/cpb.39.2225