diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

Base Information

Chemical Name:diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate
CAS No.:147909-95-3
Molecular Formula:C₃₄H₅₇NO₇
Molecular Weight:591.829
Hs Code.:

Synonyms:diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

Chemical Property:

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Technology Process of diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

There total 6 articles about diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35506-91-3,133522-25-5,136087-36-0
diethyl (4S,5S)-1,3,2-dioxathiolane-4,5-dicarboxylate 2-oxide

: 147909-95-3
diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

Guidance literature:: Multi-step reaction with 5 steps

1: NaIO₄ / RuCl₃*H₂O / CCl₄; acetonitrile; H₂O / 4 h / Ambient temperature

2: 1) NaN₃, 2) 20percent aq. H₂SO₄ / 1) acetone, water, RT, 2) ether, 16 h

3: 73 percent / iPr₂NEt / CH₂Cl₂ / 8 h / 0 deg C to RT

4: 1) Ph₃P, 2) H₂O / 1) benzene, 45 deg C, 30 min, 2) 45 deg C, 11 h

5: Et₃N, DMAP / CH₂Cl₂ / 1) 0 deg C, 1 h, 2) RT, 5 h

With dmap; sodium periodate; sodium azide; sulfuric acid; water; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; ruthenium trichloride; In tetrachloromethane; dichloromethane; water; acetonitrile;

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 147909-95-3
diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / iPr₂NEt / CH₂Cl₂ / 8 h / 0 deg C to RT

2: 1) Ph₃P, 2) H₂O / 1) benzene, 45 deg C, 30 min, 2) 45 deg C, 11 h

3: Et₃N, DMAP / CH₂Cl₂ / 1) 0 deg C, 1 h, 2) RT, 5 h

With dmap; water; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane;

Reference yield:

: 101924-62-3
1-[(1R,2S)-3-ethoxy-1-(ethoxycarbonyl)-2-hydroxy-3-oxopropyl]-1,2-triazadien-2-ium

: 147909-95-3
diethyl (2R,3S)-3-(benzyloxymethoxy)-2-(octadecanoylamino)butane-1,4-dioate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / iPr₂NEt / CH₂Cl₂ / 8 h / 0 deg C to RT

2: 1) Ph₃P, 2) H₂O / 1) benzene, 45 deg C, 30 min, 2) 45 deg C, 11 h

3: Et₃N, DMAP / CH₂Cl₂ / 1) 0 deg C, 1 h, 2) RT, 5 h

With dmap; water; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane;