N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide

Base Information

• Chemical Name: N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide
• CAS No.: 97462-66-3
• Molecular Formula: C₁₁H₁₄BrNO₂S
• Molecular Weight: 304.208
• Mol file: 97462-66-3.mol

Synonyms:N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide

Chemical Property of N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide

There total 2 articles about N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

N-allylbenzenesulfonamide (50487-70-2) + ethylene dibromide (106-93-4) → N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide (97462-66-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

DOI:10.1021/jo00350a038

Reference yield:

benzenesulfonamide (98-10-2) → N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide (97462-66-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 30 percent / K₂CO₃ / acetone / 36 h / Heating

2: 39 percent / cesium carbonate / dimethylformamide / 20 h / Ambient temperature

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide; acetone;

DOI:10.1021/jo00350a038

Reference yield: 88.0%

diphenyl diselenide (1666-13-3) + N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide (97462-66-3) → N-allyl-N-(2-phenylselanyl-ethyl)-benzenesulfonamide

Guidance literature:

diphenyl diselenide; With sodium tetrahydroborate; In ethanol;

N-2-propenyl-N-(2'-bromoethyl) benzene sulphonamide; In ethanol; for 3h; Further stages.; Heating;

DOI:10.1021/jo000128z

upstream raw materials:

N-allylbenzenesulfonamide

ethylene dibromide

benzenesulfonamide

Downstream raw materials:

N-(but-3-en-1-yl)-N-methylbenzenesulfonamide

N-(phenylsulfonyl)-3-methylpyrrolidine