2,6-dibromobenzyl methoxymethyl ether

Base Information

• Chemical Name: 2,6-dibromobenzyl methoxymethyl ether
• CAS No.: 1013031-66-7
• Molecular Formula: C₉H₁₀Br₂O₂
• Molecular Weight: 309.985
• Mol file: 1013031-66-7.mol

Synonyms:2,6-dibromobenzyl methoxymethyl ether

Chemical Property of 2,6-dibromobenzyl methoxymethyl ether

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,6-dibromobenzyl methoxymethyl ether

There total 1 articles about 2,6-dibromobenzyl methoxymethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(2,6-dibromophenyl)methanol (1013031-65-6) + chloromethyl methyl ether (107-30-2) → 2,6-dibromobenzyl methoxymethyl ether (1013031-66-7)

Guidance literature:

(2,6-dibromophenyl)methanol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2.75h;

chloromethyl methyl ether; In tetrahydrofuran; for 16h; Further stages.;

DOI:10.1039/b718763g

Reference yield: 88.0%

pyridine-2-carbaldehyde (1121-60-4) + 2,6-dibromobenzyl methoxymethyl ether (1013031-66-7) → 2-bromo-6-[1-hydroxy-1-(2-pyridyl)methyl]benzyl methoxymethyl ether (1013031-67-8)

Guidance literature:

2,6-dibromobenzyl methoxymethyl ether; With n-butyllithium; In tetrahydrofuran; pentane; at -90 ℃; for 1.3h;

pyridine-2-carbaldehyde; In tetrahydrofuran; pentane; at -90 ℃; for 1.5h; Further stages.;

DOI:10.1039/b718763g

upstream raw materials:

(2,6-dibromophenyl)methanol

chloromethyl methyl ether

Downstream raw materials:

2-bromo-6-[1-hydroxy-1-(2-pyridyl)methyl]benzyl methoxymethyl ether