3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Base Information

Chemical Name:3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol
CAS No.:1383450-05-2
Molecular Formula:C₃₀H₃₇NO₇
Molecular Weight:523.626
Hs Code.:

Synonyms:3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

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Chemical Property of 3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

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Technology Process of 3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

There total 6 articles about 3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1192755-04-6
3-O-(6'-azido-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

: 1383450-05-2
3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; at 50 ℃; for 5h;
DOI:10.1016/j.carres.2012.04.005

Reference yield:

: p-tolyl 6-azido-2,3,4-tri-O-benzyl-6-deoxy-1-thio-β-D-glucopyranoside

: 1383450-05-2
3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-iodo-succinimide / diethyl ether / 0.17 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 72 h / 20 °C / Inert atmosphere; Molecular sieve

2.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

3.1: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

With N-iodo-succinimide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; water;
DOI:10.1016/j.carres.2012.04.005

Reference yield:

: 1383449-95-3
p-tolyl 2,3,4-tri-O-benzyl-6-O-p-tosyl-1-thio-β-D-glucopyranoside

: 1383450-05-2
3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-glucopyranosyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / N,N-dimethyl-formamide / 60 °C

2.1: N-iodo-succinimide / diethyl ether / 0.17 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 72 h / 20 °C / Inert atmosphere; Molecular sieve

3.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

4.1: triphenylphosphine / tetrahydrofuran; water / 5 h / 50 °C

With N-iodo-succinimide; sodium azide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.04.005